HuagongsheHuagongshe Chemistry Print Report · For research reference only
Azido(trimethyl)stannane → HCID 58754854, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Azido(trimethyl)stannane | HCID 5104973 | — |
| Reactant | HCID 68507674 | HCID 68507674 | — |
| Product | HCID 58754854 | HCID 58754854 | — |
Reaction Steps
The title compound was prepared from 4-amino-3-cyclohex-1-enyl-benzonitrile (as prepared in the previous step, 245 mg, 0.123 mmol) and azidotrimethylstannane (267 mg, 1.29 mmol) according to the procedure in Example 52, step (c) (320 mg, 64%). Mass spectrum (ESI, m/z): Calcd. for C13H15N5, 242.1 (M-SnMe3+2H), found 242.2 (M+H).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07790724B2 |
| Source dataset | uspto-grants-2010_09 |
| ORD ID | ord-42d8e5a4024742a7aaf7b92baf8479c8 |
| Source note | uspto-grants-2010_09 |