2-Bromoaniline → HCID 58754808, compound
Reaction equation
Br[C:2]1[CH:8]=[CH:7][CH:6]=[CH:5][C:3]=1[NH2:4].[CH3:9][C:10]1([CH3:19])[CH2:15][CH2:14][C:13](B(O)O)=[CH:12][CH2:11]1>>[CH3:9][C:10]1([CH3:19])[CH2:15][CH2:14][C:13]([C:2]2[CH:8]=[CH:7][CH:6]=[CH:5][C:3]=2[NH2:4])=[CH:12][CH2:11]1Participants
3
Procedure
The title compound was prepared by Suzuki coupling of 2-bromoaniline and 4,4-dimethyl-1-cyclohexen-1-yl boronic acid according to the procedure in Example 44, step (b). Mass spectrum (ESI, m/z): Calcd. for C14H19N, 202.1 (M+H), found 202.1.
Sources & evidence
- ORD record
- ord-6a89661d37fa42b6897baafc8ac27156
- Source dataset
- uspto-grants-2010_09
- Patent number
- US07790724B2
Reaction notes
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