HuagongsheHuagongshe Chemistry Print Report · For research reference only
Hydrazine → HCID 68503406, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Hydrazine | HCID 9321 | — |
| Reactant | HCID 53823551 | HCID 53823551 | — |
| Solvent | Ethanol | HCID 702 | — |
| Product | HCID 68503406 | HCID 68503406 | — |
Reaction Steps
1-(1-Methylsulfanyl-2-nitro-vinyl)-piperidine (WO 2000016766, 202 mg, 1.00 mmol) was reacted with hydrazine (30 μL, 1.0 mmol) in EtOH to afford (2-nitro-1-piperidin-1-yl-vinyl)-hydrazine and which was converted to 4-nitro-3-piperidin-1-yl-pyridazine following procedures analogous to literature methods (Tett. Lett. 41, 3619, (1977)).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07790724B2 |
| Source dataset | uspto-grants-2010_09 |
| ORD ID | ord-3e890b06ac1542638941cf947051612a |
| Source note | uspto-grants-2010_09 |