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HRID1711733

反应详情

EQUATION

反应方程式

HRID 1711733 的结构方程式

REACTANTS

反应物

2
结构：OC1CCNCC1
HCID79341

Piperidin-4-ol

C5H11NO

结构：CC(C)Oc1ccc(S(C)(=O)=O)cc1C(=O)O
HCID21100237

2-(1-Methylethoxy)-5-(methylsulfonyl)benzoic acid

C11H14O5S

PRODUCTS

生成物

1
结构：CC(C)Oc1ccc(S(C)(=O)=O)cc1C(=O)N1CCC(O)CC1
HCID58673083

未命名化合物

收率 70%

PROCEDURE

实验过程

Prepared in analogy to Example 1 from 2-isopropoxy-5-methanesulfonyl-benzoic acid (Example A1) and 4-hydroxypiperidine. The crude material was purified by flash chromatography (methanol/dichloromethane) to yield the title compound as an amorphous yellow solid (yield 70%). MS (m/e): 342.3 (M+H+, 100%).

WORKUP

后处理

  1. customThe crude material was purified by flash chromatography (methanol/dichloromethane)