HuagongsheHuagongshe Chemie-Druckbericht · Nur für Forschungszwecke
1-Chloro-3-methoxypropane → 7-Hydroxymethyl-1-(3-methoxypropyl)-3,4-dihydro-1H-quinolin-2-one
Beteiligte Stoffe
| Rolle | Name | HCID | Einwaage |
|---|---|---|---|
| Edukt | 1-Chloro-3-methoxypropane | HCID 118927 | — |
| Edukt | 7-(Hydroxymethyl)-3,4-dihydroquinolin-2(1H)-one | HCID 53393348 | — |
| Produkt | 7-Hydroxymethyl-1-(3-methoxypropyl)-3,4-dihydro-1H-quinolin-2-one | HCID 68501224 | — |
Reaktionsschritte
Analogously to Example 2c, 1.28 g of 7-hydroxymethyl-3,4-dihydro-1H-quinolin-2-one are reacted with 1.59 ml of 1-chloro-3-methoxypropane. The title compound is obtained as a slightly yellowish oil. Rf=0.24 (dichloromethane-methanol=95:5); Rt=2.71.
Herkunft & Nachweise
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patentnummer | US07790715B2 |
| Quelldatensatz | uspto-grants-2010_09 |
| ORD ID | ord-8c6d042e6e3841cf9e4a4c20722b67d8 |
| Quellennotiz | uspto-grants-2010_09 |