1,3-Dibromopropane → HCID 10988726, compound

HRID 1712486Notes

Reaction equation

HRID 1712486 reaction equation
[F:1][C:2]1[CH:3]=[C:4]([OH:9])[CH:5]=[CH:6][C:7]=1[F:8].[Br:10][CH2:11][CH2:12][CH2:13]Br>>[Br:10][CH2:11][CH2:12][CH2:13][O:9][C:4]1[CH:5]=[CH:6][C:7]([F:8])=[C:2]([F:1])[CH:3]=1

Participants

3

Reactant 2

HCID 80011,3-DibromopropaneHCID 759273,4-Difluorophenol

Product 1

HCID 10988726HCID 10988726, compound

Procedure

Analogously to Example 91b, 2.00 g of 3,4-difluorophenol and 31.0 g of 1,3-dibromopropane are reacted. The title compound is obtained as a colourless oil. Rf=0.66 (1:6 EtOAc-heptane); Rt=5.01.

Sources & evidence

ORD record
ord-16b6a7c15909410f981f45c2e158f08c
Source dataset
uspto-grants-2010_09
Patent number
US07790715B2

Reaction notes

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