HuagongsheHuagongshe Chemistry Print Report · For research reference only
HCID 22340531, compound → HCID 68499094, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | HCID 22340531 | HCID 22340531 | — |
| Reactant | Benzyl 3-hydroxy-4-(4-hydroxyphenyl)piperidinecarboxylate | HCID 68500730 | — |
| Product | HCID 68499094 | HCID 68499094 | — |
Reaction Steps
Analogously to Method I, 9.170 g of benzyl 3-hydroxy-4-(4-hydroxyphenyl)piperidinecarboxylate and 11.00 g of tertbutyl 3-toluenesulphonyloxy)azetidine-1-carboxylate are reacted. The title compound is obtained as a yellow oil. Rf=023 (3:1 EtOAc-heptane); Rt=5.01.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07790715B2 |
| Source dataset | uspto-grants-2010_09 |
| ORD ID | ord-b93493bd349c4f4c8bd9a86574c0494e |
| Source note | uspto-grants-2010_09 |