Guaiacol → HCID 58884901, compound

HRID 1712575Notes

Reaction equation

HRID 1712575 reaction equation
[CH3:1][O:2][C:3]1[CH:8]=[CH:7][CH:6]=[CH:5][C:4]=1O.[C:10]1([CH3:33])[CH:15]=[CH:14][C:13]([S:16]([O:19][CH2:20][CH2:21][O:22]S(C2C=CC(C)=CC=2)(=O)=O)(=[O:18])=[O:17])=[CH:12][CH:11]=1>>[C:10]1([CH3:33])[CH:11]=[CH:12][C:13]([S:16]([O:19][CH2:20][CH2:21][O:22][C:5]2[CH:6]=[CH:7][CH:8]=[C:3]([O:2][CH3:1])[CH:4]=2)(=[O:17])=[O:18])=[CH:14][CH:15]=1

Participants

3

Reactant 2

HCID 460GuaiacolHCID 228289Ethylene glycol ditosylate

Product 1

HCID 58884901HCID 58884901, compound

Procedure

Analogously to Method I, 0.500 g of methoxyphenol and 4.385 g of ethylene di(p-toluenesulphonate) are reacted. The title compound is obtained as a colourless solid. Rf=0.51 (1:1 EtOAc-heptane); Rt=4.68.

Sources & evidence

ORD record
ord-005e1f11e2404b2faa4ccd808f093930
Source dataset
uspto-grants-2010_09
Patent number
US07790715B2

Reaction notes

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