HuagongsheHuagongshe Chemistry Print Report · For research reference only
Cyclopentanone → N'-cyclopentylidene(tert-butoxy)carbohydrazide
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Cyclopentanone | HCID 8452 | — |
| Reactant | tert-Butyl carbazate | HCID 70091 | — |
| Solvent | Methanol | HCID 887 | — |
| Product | N'-cyclopentylidene(tert-butoxy)carbohydrazide | HCID 4058837 | — |
Reaction Steps
A mixture of cyclopentanone (4.0 g, 47.5 mmol) and tert-butyl hydrazinecarboxylate (6.28 g, 47.5 mmol) in MeOH (100 mL) is stirred at rt for 2 hr. The solvent is removed in vacuo to yield the title compound as a white solid, which is used in the next step without further purification. MS (M+1): 199.1.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07795262B2 |
| Source dataset | uspto-grants-2010_09 |
| ORD ID | ord-874342629b0241b4b4ea806f89803c64 |
| Source note | uspto-grants-2010_09 |