Phenylboronic Acid → HCID 9834197, compound

HRID 1713285Notes

Reaction equation

Br[C:2]1[CH:9]=[CH:8][C:5]([C:6]#[N:7])=[CH:4][C:3]=1[CH3:10].[C:11]1(B(O)O)[CH:16]=[CH:15][CH:14]=[CH:13][CH:12]=1>>[CH3:10][C:3]1[CH:4]=[C:5]([CH:8]=[CH:9][C:2]=1[C:11]1[CH:16]=[CH:15][CH:14]=[CH:13][CH:12]=1)[C:6]#[N:7]

Participants

Reactant 2

HCID 66827Phenylboronic Acid

HCID 27374944-Bromo-3-methylbenzonitrile

Product 1

HCID 9834197HCID 9834197, compound

Procedure

The title compound was prepared in a similar manner to that described in Reference Example 2 using 4-bromo-3-methylbenzonitrile instead of tert-butyl N-(4-bromobenzyl)carbamate and phenylboronic acid instead of 3-benzyloxyphenylboronic acid.

Sources & evidence

ORD record: ord-c83a264aedbd440c99dc28845a53ce2e
Source dataset: uspto-grants-2010_09
DOI: 10.6084/m9.figshare.5104873.v1
Patent number: US07795236B2

Reaction notes

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