HuagongsheHuagongshe Chemistry Print Report · For research reference only
1,4-Dioxane hydrochloride → HCID 67455706, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 1,4-Dioxane hydrochloride | HCID 20443148 | — |
| Reactant | HCID 67457314 | HCID 67457314 | — |
| Product | HCID 67455706 | HCID 67455706 | — |
Reaction Steps
tert-Butyl N-(2-benzyloxy-3′-dimethylcarbamoyl-biphenyl-4-ylmethyl)carbamate (0.7 g) was suspended in 4 mol/L hydrogen chloride-1,4-dioxane solution (7.0 mL), and the resulting mixture was stirred at room temperature for 1 hour. The reaction mixture was concentrated under reduced pressure to give the title compound (0.55 g).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07795236B2 |
| Source dataset | uspto-grants-2010_09 |
| ORD ID | ord-00edabcfb64642fba583c470423978f6 |
| Source note | uspto-grants-2010_09 |