Potassium Carbonate → HCID 68506655, compound

HRID 1713391Notes

Reaction equation

HRID 1713391 reaction equation
C(=O)([O-])[O-].[K+].[K+].[C:7]([O:11][CH2:12][CH3:13])(=[O:10])[C:8]#[CH:9].C1(C)C=C(C)C=C(C)C=1S([O-])(=O)=O.[NH2:27][N+:28]1[CH:33]=[CH:32][CH:31]=[C:30]([S:34](=[O:39])(=[O:38])[N:35]([CH3:37])[CH3:36])[CH:29]=1>C(Cl)(Cl)Cl>[CH2:12]([O:11][C:7]([C:8]1[CH:9]=[N:27][N:28]2[CH:29]=[C:30]([S:34](=[O:38])(=[O:39])[N:35]([CH3:37])[CH3:36])[CH:31]=[CH:32][C:33]=12)=[O:10])[CH3:13]

Participants

5

Reactant 3

HCID 11430Potassium CarbonateHCID 12182Ethyl propiolateHCID 86625118HCID 86625118, compound

Product 1

HCID 68506655HCID 68506655, compound

Reagents, catalysts & solvents 1

HCID 6212ChloroformSolvent

Procedure

Potassium carbonate and ethyl propiolate are added to a stirred suspension of 1-Amino-3-dimethylsulfamoyl-pyridinium mesitylenesulfonate in chloroform at room temperature. For more details, see literature: Yasumitsu Tamura, Yoshio Sumida, Yasuyoshi Miki and Masazumi Ikeda, J. Chem. Soc. Perkin 1, 1974, 406-409

Sources & evidence

ORD record
ord-0d26daee8c494748a741702c6a964ca3
Source dataset
uspto-grants-2010_09
Patent number
US07795273B2

Reaction notes

Loading…