Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
3-amino-N,N-dimethylbenzylamine → HCID 18621787, 화합물
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | 3-amino-N,N-dimethylbenzylamine | HCID 99294 | — |
| 반응물 | 1-(2-(4-Isothiocyanatophenoxy)ethyl)pyrrolidine | HCID 11846122 | — |
| 반응물 | HCID 59689650 | HCID 59689650 | — |
| 반응물 | [4-(2-Pyrrolidin-1-yl-ethoxy)-phenyl]-urea | HCID 68704441 | — |
| 용매 | Dichloromethane methanol | HCID 21226129 | — |
| 생성물 | HCID 18621787 | HCID 18621787 | — |
| 생성물 | HCID 59689650 | HCID 59689650 | — |
반응 단계
The title compound is prepared as described in Example 1 for [4-(2-pyrrolidin-1-yl-ethoxy)-phenyl]-urea but using (3-isothiocyanato-benzyl)-dimethyl-amine. Title compound: ES-MS: 210.0 [M+H]+; single peak at tR=3.38 min (System 1); Rf=0.63 (CH2Cl2/MeOH, 80/20). (3-Isothiocyanato-benzyl)-dimethyl-amine is prepared as described in Example 1 for 1-[2-(4-isothiocyanato-phenoxy)ethyl]-pyrrolidine but using 3-dimethylaminomethyl-phenylamine. (3-Isothiocyanato-benzyl)dimethyl-amine is obtained and used as an impure crude material.
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US07795288B2 |
| 출처 데이터셋 | uspto-grants-2010_09 |
| ORD ID | ord-cda9356e9d114220b1e49b432a91ff9d |
| 출처 메모 | uspto-grants-2010_09 |