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HRID1713661

反应详情

EQUATION

反应方程式

HRID 1713661 的结构方程式

REACTANTS

反应物

2
结构：CN1CCN(c2ccc(NC(N)=S)cc2)CC1
HCID39146979

未命名化合物

结构：CN(C)Cc1cccc(Nc2ncc(-c3ccsc3)s2)c1
HCID58923521

未命名化合物

PRODUCTS

生成物

1
结构：CN1CCN(c2ccc(Nc3ncc(-c4ccsc4)s3)cc2)CC1
HCID58923513

未命名化合物

PROCEDURE

实验过程

The title compound is prepared as described in Example 19 for (3-dimethylaminomethyl-phenyl)-(5-thiophen-3-yl-thiazol-2-yl)-amine but starting from [4-(4-methyl-piperazin-1-yl)-phenyl]-thiourea (Example 5). MPLC (CH3CN/H2O/TFA) purification affords the title compound: ES-MS: 357.1 [M+H]+; single peak at tR=2.82 min (System 2); Rf=0.59 (CH2Cl2/MeOH, 90/10).

WORKUP

后处理

  1. customThe title compound is prepared
  2. customMPLC (CH3CN/H2O/TFA) purification