1-(3-Bromophenyl)ethanol → (3-Bromophenyl)acetaldehyde

HRID 1713666Notes

Reaction equation

HRID 1713666 reaction equation
S1[CH:5]=[CH:4][C:3]([CH2:6][CH:7]=[O:8])=[CH:2]1.[Br:9][C:10]1C=C(C(O)C)C=C[CH:15]=1>C(Cl)Cl.CCOCC>[Br:9][C:10]1[CH:2]=[C:3]([CH2:6][CH:7]=[O:8])[CH:4]=[CH:5][CH:15]=1

Participants

4

Reactant 2

HCID 984791-(3-Bromophenyl)ethanolHCID 141408302-(Thiophen-3-yl)acetaldehyde

Product 1

HCID 20387554(3-Bromophenyl)acetaldehyde

Reagents, catalysts & solvents 1

HCID 21881112Ethyl ether methylene chlorideSolvent

Procedure

The title compound is prepared as described in Example 12 (Procedure B) for 3-thiophenylacetaldehyde but using 3-bromophenyl-ethanol. The title compound: ES-MS: 196.9 [M-2]−; single peak at tR=3.89 min (System 2); Rf=0.66 (CH2Cl2/Et2O, 95/5).

Workup

  1. customThe title compound is prepared

Sources & evidence

ORD record
ord-4323ae761c9f483ea7f3090c92203ff4
Source dataset
uspto-grants-2010_09
Patent number
US07795288B2

Reaction notes

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