HuagongsheHuagongshe Chemistry Print Report · For research reference only
1-(3-Bromophenyl)ethanol → (3-Bromophenyl)acetaldehyde
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 1-(3-Bromophenyl)ethanol | HCID 98479 | — |
| Reactant | 2-(Thiophen-3-yl)acetaldehyde | HCID 14140830 | — |
| Solvent | Ethyl ether methylene chloride | HCID 21881112 | — |
| Product | (3-Bromophenyl)acetaldehyde | HCID 20387554 | — |
Reaction Steps
The title compound is prepared as described in Example 12 (Procedure B) for 3-thiophenylacetaldehyde but using 3-bromophenyl-ethanol. The title compound: ES-MS: 196.9 [M-2]−; single peak at tR=3.89 min (System 2); Rf=0.66 (CH2Cl2/Et2O, 95/5).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07795288B2 |
| Source dataset | uspto-grants-2010_09 |
| ORD ID | ord-4323ae761c9f483ea7f3090c92203ff4 |
| Source note | uspto-grants-2010_09 |