1-(2-Chlorophenyl)ethanol → 2-(2-Chlorophenyl)acetaldehyde

HRID 1713669Notes

Reaction equation

HRID 1713669 reaction equation
S1C=CC(CC=[O:8])=C1.[Cl:9][C:10]1[CH:15]=[CH:14][CH:13]=[CH:12][C:11]=1[CH:16](O)[CH3:17]>C(Cl)Cl.CCOCC>[Cl:9][C:10]1[CH:15]=[CH:14][CH:13]=[CH:12][C:11]=1[CH2:16][CH:17]=[O:8]

Participants

4

Reactant 2

HCID 260821-(2-Chlorophenyl)ethanolHCID 141408302-(Thiophen-3-yl)acetaldehyde

Product 1

HCID 113786242-(2-Chlorophenyl)acetaldehyde

Reagents, catalysts & solvents 1

HCID 21881112Ethyl ether methylene chlorideSolvent

Procedure

The title compound is prepared as described in Example 12 (Procedure B) for 3-thiophenylacetaldehyde but using 2-chlorophenyl-ethanol. The title compound: ES-MS: 152.9 [M−H]−; single peak at tR=3.82 min (System 2); Rf=0.70 (CH2Cl2/Et2O, 95/5).

Workup

  1. customThe title compound is prepared

Sources & evidence

ORD record
ord-c70de142603c450a9a7e9ebfacf61afa
Source dataset
uspto-grants-2010_09
Patent number
US07795288B2

Reaction notes

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