HuagongsheHuagongshe Chemistry Print Report · For research reference only
1-(2-Chlorophenyl)ethanol → 2-(2-Chlorophenyl)acetaldehyde
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 1-(2-Chlorophenyl)ethanol | HCID 26082 | — |
| Reactant | 2-(Thiophen-3-yl)acetaldehyde | HCID 14140830 | — |
| Solvent | Ethyl ether methylene chloride | HCID 21881112 | — |
| Product | 2-(2-Chlorophenyl)acetaldehyde | HCID 11378624 | — |
Reaction Steps
The title compound is prepared as described in Example 12 (Procedure B) for 3-thiophenylacetaldehyde but using 2-chlorophenyl-ethanol. The title compound: ES-MS: 152.9 [M−H]−; single peak at tR=3.82 min (System 2); Rf=0.70 (CH2Cl2/Et2O, 95/5).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07795288B2 |
| Source dataset | uspto-grants-2010_09 |
| ORD ID | ord-c70de142603c450a9a7e9ebfacf61afa |
| Source note | uspto-grants-2010_09 |