HuagongsheHuagongshe Chemistry Print Report · For research reference only
2-(Thiophen-3-yl)acetaldehyde → (3-Thiophen-3-yl-phenyl)-acetaldehyde
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 2-(Thiophen-3-yl)acetaldehyde | HCID 14140830 | — |
| Reactant | 2-(3-Thiophen-3-yl-phenyl)-ethanol | HCID 19917133 | — |
| Solvent | Ethyl ether methylene chloride | HCID 21881112 | — |
| Product | (3-Thiophen-3-yl-phenyl)-acetaldehyde | HCID 58923511 | — |
Reaction Steps
The title compound is prepared as described in Example 12 (Procedure B) for 3-thiophenylacetaldehyde but using 2-(3-thiophen-3-yl-phenyl)-ethanol. The title compound: ES-MS: 200.9 [M−H]−; single peak at tR=4.53 min (System 2); Rf=0.63 (CH2Cl2/Et2O, 95/5).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07795288B2 |
| Source dataset | uspto-grants-2010_09 |
| ORD ID | ord-ba154b68de2c44cb8bb2ffc9ab34776c |
| Source note | uspto-grants-2010_09 |