HuagongsheHuagongshe Chemistry Print Report · For research reference only
Methyl oxo{[4-(propylsulphonyl)phenyl]amino}acetate → 2-hydrazino-2-oxo-N-[4-(propylsulfonyl)phenyl]acetamide
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Methyl oxo{[4-(propylsulphonyl)phenyl]amino}acetate | HCID 59464270 | — |
| Reactant | HCID 178500682 | HCID 178500682 | — |
| Product | 2-hydrazino-2-oxo-N-[4-(propylsulfonyl)phenyl]acetamide | HCID 59464171 | — |
Reaction Steps
The procedure described for Intermediate 43 (part iv) was followed starting with methyl oxo{[4-(propylsulphonyl)phenyl]amino}acetate to give the title compound (Intermediate 97); 1H NMR δ 0.85-0.97 (m, 3H), 1.46-1.65 (m, 2H), 3.18-3.27 (m, 2H), 4.77 (s, 2H), 7.85 (d, 2H), 8.10 (d, 2H), 10.44 (s, 1H), 11.09 (s, 1H); MS m/e MH+ 286.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07795283B2 |
| Source dataset | uspto-grants-2010_09 |
| ORD ID | ord-62966620831e4f8dbb29044bb20e8ceb |
| Source note | uspto-grants-2010_09 |