Methyl Methacrylate → HCID 87918426, compound

Participants

Reaction Steps

A 25 ml reaction vessel was charged with 36 g ethyl acetate, 2.15 g (0.005 mol) TRIS, 1.58 g (0.016 mol) methyl methacrylate, 0.32 g (0.003 mol) NIPAM, and 0.078 g. 2,2′-azobis(2-methylbutanenitrile). After nitrogen flushing for 3 minutes, the vessel was closed and placed in an oil bath. The polymerization was run for 18 hours at 61-65° C. The polymer was precipitated into water and dried at room temperature (20° C.). The polymer was soluble in HMDS.

Provenance & Evidence