反应详情

Methyl 1-but-3-en-1-yl-3-cyclohexyl-2-(2-vinylphenyl)-1H-indole-6-carboxylate was dissolved in DCM (0.02M) and treated with Zhan catalyst 1 (0.3 eq) at 35° C. for 1 h. After evaporation of solvent in vacuo the residue was purified by chromatography (PE/EtOAc 9:1) to afford the title compound (68%); MS (ES+) m/z 386 (M+H)+.

1. customAfter evaporation of solvent in vacuo the residue
2. customwas purified by chromatography (PE/EtOAc 9:1)