HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 1714133Generated: November 2, 2026
HCID 16117409, compound → HCID 16117410, compound
https://huagongshe.com/reaction/1714133
Participants
| Role | Name | HCID | Charge |
|---|
| Reactant | HCID 16117409 | HCID 16117409 | — |
| Catalyst | Palladium hydroxide | HCID 9942167 | — |
| Solvent | Methanol | HCID 887 | — |
| Product | HCID 16117410 | HCID 16117410 | — |
Reaction Steps
To a solution of cis-3-benzyl-6-(2,4-dichloro-phenyl)-1,2,3,4,4a,9a-hexahydro-3-aza-fluoren-9-one (132 mg, 0.31 mmol) in MeOH (4.0 mL) was added Pd(OH)2 (26 mg, 20 wt %). The reaction mixture was stirred at 20° C. for 15 h under H2 atmosphere, filtered through celite and concentrated in vacuo to give the crude title compound.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
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| Patent number | US07795436B2 |
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| Source dataset | uspto-grants-2010_09 |
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| ORD ID | ord-95046f51d75a47c3afd9c27ad8218887 |
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| Source note | uspto-grants-2010_09 |
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