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HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 1714133Generated: November 2, 2026

HCID 16117409, compound → HCID 16117410, compound

https://huagongshe.com/reaction/1714133

Reaction equation

Participants

RoleNameHCIDCharge
ReactantHCID 16117409HCID 16117409—
CatalystPalladium hydroxideHCID 9942167—
SolventMethanolHCID 887—
ProductHCID 16117410HCID 16117410—

Reaction Conditions

Temperature20 °C

Reaction Steps

To a solution of cis-3-benzyl-6-(2,4-dichloro-phenyl)-1,2,3,4,4a,9a-hexahydro-3-aza-fluoren-9-one (132 mg, 0.31 mmol) in MeOH (4.0 mL) was added Pd(OH)2 (26 mg, 20 wt %). The reaction mixture was stirred at 20° C. for 15 h under H2 atmosphere, filtered through celite and concentrated in vacuo to give the crude title compound.

Provenance & Evidence

DOI10.6084/m9.figshare.5104873.v1
Patent numberUS07795436B2
Source datasetuspto-grants-2010_09
ORD IDord-95046f51d75a47c3afd9c27ad8218887
Source noteuspto-grants-2010_09