Triethylsilane → HCID 16117411, compound

Participants

Reaction Conditions

Reaction Steps

To a solution of cis-6-(2,4-dichloro-phenyl)-1,2,3,4,4a,9a-hexahydro-3-aza-fluoren-9-one (40 mg, 0.12 mmol) in trifluoroacetic acid (2.0 mL) was added Et3SiH (62 mg, 0.53 mmol). The reaction mixture was stirred at 20° C. for 15 h then concentrated in vacuo. The residue was basified with NH4OH then extracted with CH2Cl2. The organic layer was dried over MgSO4, filtered and concentrated in vacuo to give the crude title compound.

Provenance & Evidence