HuagongsheHuagongshe Chemistry Print Report · For research reference only
HCID 16117541, compound → HCID 16117542, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | HCID 16117541 | HCID 16117541 | — |
| Catalyst | Palladium hydroxide | HCID 9942167 | — |
| Solvent | Methanol | HCID 887 | — |
| Product | HCID 16117542 | HCID 16117542 | — |
Reaction Steps
The title compound was prepared as a white solid (69 mg, 0.21) by following the procedure step A of example 4 from cis-3-benzyl-8-(2,4-dichloro-phenyl)-1,2,3,4,4a,9a-hexahydro-3-aza-fluoren-9-one (90 mg, 0.21 mmol) and Pd(OH)2 (18 mg, 20 wt %) in MeOH (3.0 mL): MS (ES) 332.1 (M+H).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07795436B2 |
| Source dataset | uspto-grants-2010_09 |
| ORD ID | ord-f77422a6b0184566ba3ccb96c876d31f |
| Source note | uspto-grants-2010_09 |