HRID1714181
反应详情
EQUATION
反应方程式
REACTANTS
反应物
PRODUCTS
生成物
AUXILIARIES
试剂、催化剂与溶剂
PROCEDURE
实验过程
33 mg (0.07 mmol) of tert-butyl {3-[6-benzoylamino-1-(3-methylbut-2-enyl)-1H-benzimidazol-2-ylsulfanyl]propyl}carbamate were dissolved in 102 μl of trifluoroacetic acid and 100 μl of water and stirred at room temperature for 6 hours. The reaction mixture was diluted with water and freeze-dried. 34 mg of the desired product were obtained in quantitative yield.
WORKUP
后处理
- customfreeze-dried