HuagongsheHuagongshe Chemistry Print Report · For research reference only
Hydrochloric Acid → HCID 178453906, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Hydrochloric Acid | HCID 313 | — |
| Reactant | Sodium triacetoxyborohydride | HCID 5049666 | — |
| Reactant | HCID 63674670 | HCID 63674670 | — |
| Reactant | HCID 178453924 | HCID 178453924 | — |
| Solvent | 1,2-Dichloroethane | HCID 11 | — |
| Product | HCID 178453906 | HCID 178453906 | — |
Reaction Steps
The title compound was prepared analogously to example 1 (1.3) starting from 5-Fluoro-2-(piperidin-4-yloxy)-benzonitrile; hydrochloride and Trans-[4-(2-Oxo-ethyl)-cyclohexyl]-carbamic acid tert-butyl ester with sodium triacetoxyborohydride in 1,2-dichloroetane. MS (m/e): 446.3 (M+H+)
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07795437B2 |
| Source dataset | uspto-grants-2010_09 |
| ORD ID | ord-6044bf1e29ca4c1aa5f00bb892a725e1 |
| Source note | uspto-grants-2010_09 |