HuagongsheHuagongshe Chemistry Print Report · For research reference only
Benzylamine → HCID 178502581, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Benzylamine | HCID 7504 | — |
| Reactant | HCID 178502582 | HCID 178502582 | — |
| Solvent | Toluene | HCID 1140 | — |
| Product | HCID 178502581 | HCID 178502581 | 91% |
Reaction Steps
Sodium sulfate anhydride (120 mg) was added to a solution obtained by dissolving 3-(methoxymethylphosphinyl)-propanal (60 mg) and benzylamine (42.8 mg) in toluene (3 ml), then the resultant solution was stirred for an hour at room temperature. Sodium sulfate was filtered out, and the resultant filtrate was concentrated to obtain N-benzyl-3-(methoxymethylphosphinyl)-propylideneamine (87 mg).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07795464B2 |
| Source dataset | uspto-grants-2010_09 |
| ORD ID | ord-d7b5dd0b063949499b86205db004b0b4 |
| Source note | uspto-grants-2010_09 |