HuagongsheHuagongshe Chemistry Print Report · For research reference only
Hydrochloric Acid → HCID 23642228, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Hydrochloric Acid | HCID 313 | — |
| Reactant | HCID 68507399 | HCID 68507399 | — |
| Solvent | Diethyl Ether | HCID 3283 | — |
| Product | HCID 23642228 | HCID 23642228 | — |
Reaction Steps
A solution of 0.245 g (0.6 mmoles) (6-benzenesulfonyl-naphthalen-1-ylmethyl)-methyl-carbamic acid tert-butyl ester and 20 mL 2 M hydrogen chloride in ethyl ether was stirred at 23° C. for 20 hours. The resulting white solid was collected by filtration and dried in vacuo to provide (6-benzenesulfonyl-naphthalen-1-ylmethyl)-methyl-amine as a hydrochloride salt, 0.12 gram (57%), M+H=312.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07799797B2 |
| Source dataset | uspto-grants-2010_09 |
| ORD ID | ord-9499dda1bbc84c7f869c8b4b712fe9d9 |
| Source note | uspto-grants-2010_09 |