Dimethylformamide dimethyl acetal → HCID 59028789, compound

Participants

Reaction Conditions

Reaction Steps

C-(6-Benzenesulfonyl-naphthalen-1-yl)-methylamine is added to dimethylformamide dimethyl acetal, and the reaction mixture is heated to 95° C. The reaction mixture is cooled and quenched by addition of water, and the resulting aqueous mixture is extracted with EtOAc. The organic layer is washed with water, brine, dried (MgSO4), and evaporated under reduced pressure to give N′-(6-Benzenesulfonyl-naphthalen-1-ylmethyl)-N,N-dimethyl-formamidine.

Provenance & Evidence