HRID1715062

反应详情

EQUATION

反应方程式

HRID 1715062 的结构方程式

AUXILIARIES

试剂、催化剂与溶剂

1

PROCEDURE

实验过程

C-(6-Benzenesulfonyl-naphthalen-1-yl)-methylamine is dissolved in pyridine and acetyl chloride is added. The reaction mixture is stirred at room temperature and then quenched by addition of water. The mixture is extracted with EtOAc, and the organic layer is dried (MgSO4), filtered, and concentrated under reduced pressure to give N-(6-benzenesulfonyl-naphthalen-1-ylmethyl)-acetamide.

WORKUP

后处理

  1. customquenched by addition of water
  2. extractionThe mixture is extracted with EtOAc
  3. dry with materialthe organic layer is dried (MgSO4)
  4. filtrationfiltered
  5. concentrationconcentrated under reduced pressure