HuagongsheHuagongshe Chemistry Print Report · For research reference only
Methylamine → HCID 59028782, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Methylamine | HCID 6329 | — |
| Reactant | HCID 59028781 | HCID 59028781 | — |
| Solvent | Methanol | HCID 887 | — |
| Product | HCID 59028782 | HCID 59028782 | — |
Reaction Steps
[(6-Benzenesulfonyl-naphthalen-1-ylmethyl)-amino]-acetic acid ethyl ester is added to methylamine in methanol, and the solution is stirred at room temperature, then concentrated under reduced pressure. The oil is dissolved in ethanol and 1N HCl in diethyl ether is added to precipitate 2-[(6-benzenesulfonyl-naphthalen-1-ylmethyl)-amino]-N-methyl-acetamide as a hydrochloride salt.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07799797B2 |
| Source dataset | uspto-grants-2010_09 |
| ORD ID | ord-734053a8563941c48289a84ce57d8544 |
| Source note | uspto-grants-2010_09 |