Methanol → HCID 68506502, compound

Participants

Reaction Steps

To a stirred solution of [2-(5-methyl-isoxazol-3-ylcarbamoyl)-ethyl]-carbamic acid tert-butyl ester (0.1 g, 0.37 mmol) in MeCN (3 ml) is added dropwise TMSI (0.11 ml, 0.74 mmol). After 30 minutes, MeOH (1 ml) is added to afford a yellow suspension which is collected by filtration and washed with EtOAc to afford the title compound. Further product is obtained by concentration of the filtrate.

Provenance & Evidence