Acetic Acid → HCID 23146832, compound

Participants

Reaction Steps

10.1 g (82 mmol) of 1,2,3-triaminobenzene and 14.6 g (70 mmol) of 9,10-phenanthrenequinone were placed in a four-necked flask, to which 350 g of a solvent of acetic acid and methanol at 1:1 was added for dissolution, followed by reaction at a reaction temperature of 70° C. for 2 hours. After the reaction, the solvent was removed and the resulting product was washed with methanol to obtain the intended product.

Provenance & Evidence