HCID 86612732, compound → HCID 86612731, compound

Participants

Reaction Steps

4.5 g (10.8 mmol) of N-4-nitrophenyl-10-aminodibenzo(A,C)phenazine was dissolved in 200 ml of tetrahydrofuran, and the reaction container was purged with nitrogen. Thereafter, 4.6 g of 5% Pd/C (hydrous) was added, followed by sufficient purging with nitrogen again. This system was purged with hydrogen, followed by reaction at room temperature for 10 hours. After completion of the reaction, the system was filtered, and the resulting filtration residue was further washed with tetrahydrofuran and purified with a column to obtain the intended product.

Provenance & Evidence