Hydrochloric Acid → HCID 86594427, compound

HRID 1715638Notes

Reaction equation

HRID 1715638 reaction equation
[CH3:1][O:2][C:3](=[O:21])[C@@H:4]([NH:13]C(OC(C)(C)C)=O)[CH2:5][CH2:6][N:7]([CH2:9][CH2:10][O:11][CH3:12])[CH3:8].[ClH:22]>>[ClH:22].[ClH:22].[CH3:1][O:2][C:3](=[O:21])[C@@H:4]([NH2:13])[CH2:5][CH2:6][N:7]([CH2:9][CH2:10][O:11][CH3:12])[CH3:8]

Participants

3

Reactant 2

HCID 313Hydrochloric AcidHCID 86594426HCID 86594426, compound

Product 1

HCID 86594427HCID 86594427, compound

Procedure

(S)-2-tert-Butoxycarbonylamino-4-[(2-methoxyethyl)-methylamino]-butyric acid methyl ester (0.086 g, 0.28 mmol) was treated with HCl (1 mL of 4M in dioxane) and sonicated. The mixture was concentrated and dried under high vacuum to provide the product.

Workup

  1. customsonicated
  2. concentrationThe mixture was concentrated
  3. customdried under high vacuum
  4. customto provide the product

Sources & evidence

ORD record
ord-aef2eacb093347ce8dd912a7062b2d64
Source dataset
uspto-grants-2010_09
Patent number
US07799782B2

Reaction notes

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