HRID1715795

反应详情

EQUATION

反应方程式

HRID 1715795 的结构方程式

AUXILIARIES

试剂、催化剂与溶剂

2

PROCEDURE

实验过程

The mixture of 6 g of 2-nitro-5-(morpholin-4-yl)benzoic acid, 15 mL of cyclohexene and 3 g of Pd/C (10%) is heated under reflux conditions in 120 mL of ethanol for 6 hours. The hot reaction mixture is filtered through celite filter. The filtrate is evaporated to obtain 4.8 g of the title compound. m.p.: 242° C.

WORKUP

后处理

  1. filtrationThe hot reaction mixture is filtered through celite filter
  2. customThe filtrate is evaporated