HuagongsheHuagongshe Chemistry Print Report · For research reference only
Benzylamine → 2-Amino-3-cyano-4-benzalamino-6-dimethylaminoquinoline
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Benzylamine | HCID 7504 | — |
| Reactant | 2-Amino-3-cyano-4-chloro-6-dimethylaminoquinoline | HCID 66850378 | — |
| Solvent | Water | HCID 962 | — |
| Product | 2-Amino-3-cyano-4-benzalamino-6-dimethylaminoquinoline | HCID 67523708 | — |
Reaction Steps
3 g of 2-amino-3-cyano-4-chloro-6-dimethylaminoquinoline and 6 mL of benzylamine are stirred at 125° C. for 3 hours. The reaction mixture is poured onto 30 mL of water. The precipitated material is filtered off, washed with 20 mL of water. After drying 2.3 g of the title compound is obtained, m.p.: 265° C.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07799922B2 |
| Source dataset | uspto-grants-2010_09 |
| ORD ID | ord-70551868b4ae448e98f95fbb64feef30 |
| Source note | uspto-grants-2010_09 |