Participants
| Role | Name | HCID | Charge |
|---|
| Reactant | Phenol | HCID 996 | — |
| Reactant | Sulfuric Acid | HCID 1118 | — |
| Reactant | Sodium Hydroxide | HCID 14798 | — |
| Reactant | HCID 57864781 | HCID 57864781 | — |
| Product | HCID 57864775 | HCID 57864775 | 76% |
Reaction Steps
10 parts by weight of tris(4-iodophenyl)methanol, 4.4 parts by weight of phenol, and 2 parts by weight of conc. sulfuric acid were put into a reaction vessel and stirred for 4 hours while heating at 80° C. After cooling, a 10% sodium hydroxide solution was added to the reaction solution, and stirring was carried out for 2 hours. A deposited precipitate was collected by filtration, thus giving 8.5 parts by weight of 4-hydroxyphenyl[tris(4-iodophenyl)]methane (yield: 76%).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|
| Patent number | US07799949B2 |
|---|
| Source dataset | uspto-grants-2010_09 |
|---|
| ORD ID | ord-df3027df42944689b80e8a0e38a554d6 |
|---|
| Source note | uspto-grants-2010_09 |
|---|
