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HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 1715874Generated: November 2, 2026

Aniline → HCID 57864785, compound

https://huagongshe.com/reaction/1715874

Reaction equation

Participants

RoleNameHCIDCharge
ReactantAnilineHCID 6115—
ReactantHCID 57864781HCID 57864781—
SolventEthanolHCID 702—
ProductHCID 57864785HCID 5786478593%

Reaction Conditions

Temperature190 °C

Reaction Steps

89 parts by weight of tris(4-iodophenyl)methanol and 500 parts by weight of aniline were put into a reaction vessel and stirred for 4 hours while heating at 190° C. 350 parts by weight of ethanol was added thereto, and stirring was carried out for 1 hour while heating at 90° C. After cooling, a deposited solid was collected by filtration and washed with methanol, thus giving 100 parts by weight of 4-aminophenyl[tris(4-iodophenyl)]methane (yield: 93%).

Provenance & Evidence

DOI10.6084/m9.figshare.5104873.v1
Patent numberUS07799949B2
Source datasetuspto-grants-2010_09
ORD IDord-ca0308c1eb54413ab9454931e69eb30e
Source noteuspto-grants-2010_09