Participants
| Role | Name | HCID | Charge |
|---|
| Reactant | Aniline | HCID 6115 | — |
| Reactant | HCID 57864781 | HCID 57864781 | — |
| Solvent | Ethanol | HCID 702 | — |
| Product | HCID 57864785 | HCID 57864785 | 93% |
Reaction Steps
89 parts by weight of tris(4-iodophenyl)methanol and 500 parts by weight of aniline were put into a reaction vessel and stirred for 4 hours while heating at 190° C. 350 parts by weight of ethanol was added thereto, and stirring was carried out for 1 hour while heating at 90° C. After cooling, a deposited solid was collected by filtration and washed with methanol, thus giving 100 parts by weight of 4-aminophenyl[tris(4-iodophenyl)]methane (yield: 93%).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
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| Patent number | US07799949B2 |
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| Source dataset | uspto-grants-2010_09 |
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| ORD ID | ord-ca0308c1eb54413ab9454931e69eb30e |
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| Source note | uspto-grants-2010_09 |
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