HuagongsheHuagongshe Chemistry Print Report · For research reference only
4-Aminobenzoic Acid → Carbamazepine 4-aminobenzoic acid
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 4-Aminobenzoic Acid | HCID 978 | — |
| Reactant | Carbamazepine | HCID 2554 | — |
| Solvent | Methanol | HCID 887 | — |
| Product | Carbamazepine 4-aminobenzoic acid | HCID 68425507 | — |
Reaction Steps
40 mg (0.1693 mmol) of carbamazepine and 30 mg (0.1421 mmol) of 4-aminobenzoic acid were dissolved in approximately 3 mL methanol. Slow evaporation of the solvent yielded clear plates of carbamazepine:4-aminobenzoic acid (2:1) co-crystal. The co-crystal was analyzed via IR spectroscopy and single-crystal x-ray diffraction.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07803786B2 |
| Source dataset | uspto-grants-2010_09 |
| ORD ID | ord-44bb3b9cb73747d187051a5a3f9e2af5 |
| Source note | uspto-grants-2010_09 |