HCID 59467988, compound → HCID 44455124, compound

Participants

Reaction Steps

A solution of (R)—N-(1-benzyloxy-2-oxo-piperidin-3-yl)-4-(4-chloro-phenoxy)-benzenesulfonamide (0.1 g) in step A in MeSO3H (1.5 mL) was stirred at room temperature under N2 for 16 h. The reaction was quenched with ice-water and the precipitate was filtered. The white solid was washed with water, Et2O/hexanes (1:5) to give the titled compound. MS (EI) 397 (M+H)+.

Provenance & Evidence