(4-Methoxyphenyl)boronic acid → HCID 68512694, compound

HRID 1716311Notes

Reaction equation

HRID 1716311 reaction equation
[CH2:1]([O:8][C:9]1[C:10](=[O:26])[N:11]([CH2:15][S:16]([C:19]2[CH:24]=[CH:23][C:22](Br)=[CH:21][CH:20]=2)(=[O:18])=[O:17])[CH:12]=[CH:13][CH:14]=1)[C:2]1[CH:7]=[CH:6][CH:5]=[CH:4][CH:3]=1.[CH3:27][O:28][C:29]1[CH:34]=[CH:33][C:32](B(O)O)=[CH:31][CH:30]=1>>[CH2:1]([O:8][C:9]1[C:10](=[O:26])[N:11]([CH2:15][S:16]([C:19]2[CH:24]=[CH:23][C:22]([C:32]3[CH:33]=[CH:34][C:29]([O:28][CH3:27])=[CH:30][CH:31]=3)=[CH:21][CH:20]=2)(=[O:18])=[O:17])[CH:12]=[CH:13][CH:14]=1)[C:2]1[CH:7]=[CH:6][CH:5]=[CH:4][CH:3]=1

Participants

3

Reactant 2

HCID 201262(4-Methoxyphenyl)boronic acidHCID 68517173HCID 68517173, compound

Product 1

HCID 68512694HCID 68512694, compound

Procedure

The titled compound was prepared from 3-benzyloxy-1-(4-bromo-benzenesulfonylmethyl)-1H-pyridin-2-one (obtained from Example 65) and 4-methoxy-phenylboronic acid according to the procedure described in Example 52 Step A. MS: 462 (M+H).

Sources & evidence

ORD record
ord-6d35bb5366044826ad5735637fedab39
Source dataset
uspto-grants-2010_09
Patent number
US07803793B2

Reaction notes

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