HuagongsheHuagongshe Chemistry Print Report · For research reference only
Methanol → Methyl 6-chloro-1H-indole-3-carboxylate
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Methanol | HCID 887 | — |
| Reactant | 6-chloro-1H-indole-3-carboxylic acid | HCID 18453235 | — |
| Catalyst | Sulfuric Acid | HCID 1118 | — |
| Product | Methyl 6-chloro-1H-indole-3-carboxylate | HCID 49108265 | — |
Reaction Steps
1 g of 6-chloro-1H-indole-3-carboxylic acid were heated at reflux in MeOH with 3 drop of concentrated H2SO4 overnight. Concentration in vacuo afforded the title compound in quantitative yield.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07803815B2 |
| Source dataset | uspto-grants-2010_09 |
| ORD ID | ord-42a61e3d939f4304bc7bb329142fb84e |
| Source note | uspto-grants-2010_09 |