HuagongsheHuagongshe Chemistry Print Report · For research reference only
Methyl 4-(1H-benzo[d]imidazol-2-yl)benzoate → HCID 57550190, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Methyl 4-(1H-benzo[d]imidazol-2-yl)benzoate | HCID 2328806 | — |
| Reactant | (S)-methyl 2-amino-3-hydroxypropanoate | HCID 2723731 | — |
| Product | HCID 57550190 | HCID 57550190 | — |
Reaction Steps
Using essentially the same procedures described in Examples 23 and 24 and employing methyl 4-(1-H-benzimidazol-2-yl)benzoate and serine methyl ester as starting materials the title compound was obtained and identified by NMR and mass spectral analyses. 1HNMR (400 MHz, DMSO-d6): 3.86 (s, 3H), 7.22-7.24 (m, 2H), 7.62 (d, J=3.2 Hz, 2H), 8.19 (d, J=7.6 Hz, 2H), 8.36 (d, J=8 Hz, 2H), 9.02 (s, 1H), 13.1 (s, 1H). LCMS (ESI+) 319 (MH+).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07803825B2 |
| Source dataset | uspto-grants-2010_09 |
| ORD ID | ord-9af8a364a6d54e85a5b7735bdaa16204 |
| Source note | uspto-grants-2010_09 |