HuagongsheHuagongshe Chemistry Print Report · For research reference only
Hydrochloric Acid → HCID 68510512, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Hydrochloric Acid | HCID 313 | — |
| Reactant | HCID 68513412 | HCID 68513412 | — |
| Solvent | Methanol | HCID 887 | — |
| Solvent | Isopropanol | HCID 3776 | — |
| Product | HCID 68510512 | HCID 68510512 | — |
Reaction Steps
Pyrrolidin-3-yl-carbamic acid tert-butyl ester (9) (0.25 g, 1.00 mmol, 1 equiv) was dissolved in methanol (50 mL), followed by the addition of 5-6 N HCl in isopropanol (10 mL). The solution was stirred at room temperature for 24 h. The solution was evaporated under reduced pressure to give the title compound (0.22 g, 1.00 mmol, quantitative).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07803836B2 |
| Source dataset | uspto-grants-2010_09 |
| ORD ID | ord-55ff6e82c56847538653adf6232cd770 |
| Source note | uspto-grants-2010_09 |