HRID1717060

反应详情

EQUATION

反应方程式

HRID 1717060 的结构方程式

PROCEDURE

实验过程

5-(3-Chloro-phenyl)-furan-2-carboxylic acid (65) (54 mg, 0.24 mmol) was coupled to ethyl ester (58) (50 mg, 0.24 mmol) using Method C. The crude residue was purified by column chromatography eluting with 20% EtOAc in heptane to give the title compound.

WORKUP

后处理

  1. customThe crude residue was purified by column chromatography
  2. washeluting with 20% EtOAc in heptane