HuagongsheHuagongshe Chemistry Print Report · For research reference only
5-(3,5-Dichlorophenyl)furan-2-carboxylic acid → 5-(3,5-Dichloro-phenyl)-furan-2-carboxylic acid (3-cyanomethyl-phenyl)-amide
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 5-(3,5-Dichlorophenyl)furan-2-carboxylic acid | HCID 4066369 | — |
| Reactant | (3-Amino-phenyl)-acetonitrile | HCID 4847850 | — |
| Product | 5-(3,5-Dichloro-phenyl)-furan-2-carboxylic acid (3-cyanomethyl-phenyl)-amide | HCID 59654720 | — |
Reaction Steps
Carboxylic acid (67) (62 mg, 0.24 mmol) was coupled to aniline (80) (32 mg, 0.24 mmol) using Method C. After work-up, the solid was recrystallised from MeCN (3 ml) to give the title compound.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07803841B2 |
| Source dataset | uspto-grants-2010_09 |
| ORD ID | ord-0edc002a353245bdaa66fd3036b99c57 |
| Source note | uspto-grants-2010_09 |