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HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 1717224Generated: November 2, 2026

Acetic Acid → HCID 23146832, compound

https://huagongshe.com/reaction/1717224

Reaction equation

Participants

RoleNameHCIDCharge
ReactantAcetic AcidHCID 176—
Reactant9,10-PhenanthrenedioneHCID 6763—
Reactant1,2,3-BenzenetriamineHCID 69099—
SolventMethanolHCID 887—
ProductHCID 23146832HCID 23146832—

Reaction Steps

10.1 g (82 mmol) of 1,2,3-triaminobenzene and 4.6 g (70 mmol) of 9,10-phenanthrenequinone were placed in a four-necked flask, to which 350 g of a solvent of acetic acid and methanol at 1:1 was added for dissolution, followed by reaction at a reaction temperature of 70° C. for 2 hours. After the reaction, the solvent was removed and the resulting product was washed with methanol to obtain the intended product.

Provenance & Evidence

DOI10.6084/m9.figshare.5104873.v1
Patent numberUS07803898B2
Source datasetuspto-grants-2010_09
ORD IDord-48038dfde12b41a18a43c9eb84f81904
Source noteuspto-grants-2010_09