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HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 1717239Generated: November 2, 2026

Hydrochloric Acid → HCID 68514994, compound

https://huagongshe.com/reaction/1717239

Reaction equation

Participants

RoleNameHCIDCharge
ReactantHydrochloric AcidHCID 313—
ReactantHCID 86629792HCID 86629792—
SolventEthanolHCID 702—
SolventIsopropanolHCID 3776—
ProductHCID 68514994HCID 68514994108.8%

Reaction Steps

To a suspension of tert-butyl {2-[(4-{4-[(cyclopropylamino)carbonyl]-5-propyl-1H-1,2,3-triazol-1-yl}phenyl)amino]-2-oxoethyl}carbamate (0.76 g) obtained in Example 22 in ethanol (5 ml) was added 6N hydrochloric acid in isopropyl alcohol solution (6 ml) at room temperature, and the mixture was stirred for 2 hr. The solvent was evaporated under reduced pressure to give the title compound as a white powder (0.64 g, 100%).

Provenance & Evidence

DOI10.6084/m9.figshare.5104873.v1
Patent numberUS07803822B2
Source datasetuspto-grants-2010_09
ORD IDord-abcea3c4ef8f4f948a10acfe9d5fea63
Source noteuspto-grants-2010_09