HuagongsheHuagongshe Chemistry Print Report · For research reference only
Hydrochloric Acid → HCID 68514994, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Hydrochloric Acid | HCID 313 | — |
| Reactant | HCID 86629792 | HCID 86629792 | — |
| Solvent | Ethanol | HCID 702 | — |
| Solvent | Isopropanol | HCID 3776 | — |
| Product | HCID 68514994 | HCID 68514994 | 108.8% |
Reaction Steps
To a suspension of tert-butyl {2-[(4-{4-[(cyclopropylamino)carbonyl]-5-propyl-1H-1,2,3-triazol-1-yl}phenyl)amino]-2-oxoethyl}carbamate (0.76 g) obtained in Example 22 in ethanol (5 ml) was added 6N hydrochloric acid in isopropyl alcohol solution (6 ml) at room temperature, and the mixture was stirred for 2 hr. The solvent was evaporated under reduced pressure to give the title compound as a white powder (0.64 g, 100%).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07803822B2 |
| Source dataset | uspto-grants-2010_09 |
| ORD ID | ord-abcea3c4ef8f4f948a10acfe9d5fea63 |
| Source note | uspto-grants-2010_09 |